Test of VT pBN heater plate
- Remove old sample, re-attach top plate, verify thickness of assembly and heater brushes
- 7.6 mm total, 2.9-3.0 from top of brush to bottom of top plate
- 17 ohm left brush (seen from handle) to ground. Right brush grounded.
- Sample Heating Selector to "Direct Current"
- Initial 1.6 V at 0.16 A (10 ohm), gentle pressure rise, manipulator TC increases linearly with time 22 to 28 C over 6 minutes, 0.25 W
- Next 3.24 V 0.40 A 1.3 W 8.1 Ohm
- 4.49 V 0.65 A 2.96 W 6.7 Ohm, temp rises slowly with time
- 5.73 V, 1.04 A, 5.96 W 5.7 Ohm, current rises to 1.18, pressure low 1e7 outgassing
- More tests
- Set 6.26 V 1.05 A Monday 9:23 am
- by 10:14 current limited at 1.49 A, 5.7s C 8.5 W, stage at 270 C
- pressure rose to 1e-7 then down to 2e-9
- increase current to 2.01 A, initial 7.43 V drops to 7.23 steady state, 14.5 W
- stage steady state 332 C. pBN heater uniform "cherry red"
- contact bars also hot, darker red
- heat shield, top plate, sample straps do not glow
- pressure has dropped to 1e-9
- Set 1.49 A, 5.55 V increases to 5.70, initially 3.72 Ohm -> 3.83
- heater "incipient red" just at visible glow threshold
- steady state base 280 C
- 8.5 W
|
Photo of heater at 14.5 Watts, pBN "cherry red" |
|
Approximate sample temp vs power for pBN VT holders |
No comments:
Post a Comment